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創(chuàng)見(jiàn)|實(shí)干|卓越
與光同程,，做民族儀器企業(yè)
泊菲萊科技
關(guān)閉

光解水water-splitting reaction

Labsolar-6A 全玻璃自動(dòng)在線微量氣體分析系統(tǒng)

Labsolar-6a All-glass automatic on-line trace gas analysis system

產(chǎn)品中心：光解水品牌：泊菲萊瀏覽量：60604
Labsolar-6A 全玻璃自動(dòng)在線微量氣體分析系統(tǒng)集成控制程序,，操作簡(jiǎn)單方便,，強(qiáng)大的兼容性,，可通過(guò)更換不同的反應(yīng)器實(shí)現(xiàn)光催化,、光熱催化,、電催化,、PEC光電化學(xué)等反應(yīng)的微量氣體檢測(cè),。
  • 產(chǎn)品介紹
  • 應(yīng)用領(lǐng)域
  • 文獻(xiàn)
  • 技術(shù)維護(hù)

關(guān)鍵特征

● 玻璃閥+自動(dòng)執(zhí)行器,，實(shí)現(xiàn)氣密性與效率兼顧的目標(biāo),；

● 高效氣體循環(huán)，既有效促進(jìn)反應(yīng)與催化劑之間的傳質(zhì)作用,，又有效避免因產(chǎn)物分子的重吸附作用引發(fā)的副反應(yīng)和逆反應(yīng),，準(zhǔn)確呈現(xiàn)催化劑的本征活性；

● 氣體快速混合,，氣體混勻時(shí)間<10 min,，確保產(chǎn)物檢測(cè)的準(zhǔn)確性；

● 集成控制程序,，操作簡(jiǎn)單方便,，準(zhǔn)確性達(dá)科學(xué)級(jí)水準(zhǔn)；

● 強(qiáng)大的兼容性,，可通過(guò)更換不同的反應(yīng)器實(shí)現(xiàn)光催化,、光熱催化,、電催化、PEC光電化學(xué)等反應(yīng)的微量氣體檢測(cè),。

 

應(yīng)用領(lǐng)域

▲特別適用   ●較為適用  ○可以使用

▲ 光催化/光電催化分解水制氫/氧

▲ 光催化/光電催化全分解水

▲ 光催化/光電催化CO2還原

▲ 光催化量子效率測(cè)量

▲ 光熱催化（負(fù)壓常壓體系）

▲ 電催化HER,、OER、CO2RR

 

可搭配多種反應(yīng)器拓展應(yīng)用

 

氣體循環(huán)參數(shù)

●氣體混勻時(shí)間：H2,、O2、CH4,、CO混勻時(shí)間<10 min,；

●標(biāo)準(zhǔn)曲線線性：H2含量為100 μL~10 mL范圍時(shí)，R2>0.9995;

●重復(fù)性：同一濃度連續(xù)四次進(jìn)樣,，RSD<3%;

●排氣量 ：6 mL/次,，負(fù)壓至常壓均能提供優(yōu)異的循環(huán)驅(qū)動(dòng)力;

●無(wú)源磁驅(qū)柱塞泵：管路中無(wú)電線接入，無(wú)氫爆風(fēng)險(xiǎn),，不產(chǎn)生電解水析氫干擾,；具有單向閥結(jié)構(gòu)，可實(shí)現(xiàn)所有管路的單向循環(huán);

●取樣方式：定量環(huán)位于多通玻璃取樣閥,，非色譜取樣;

●循環(huán)管路:最窄管路為內(nèi)徑為3 mm,，非小口徑色譜管路，氣體阻力小

外觀結(jié)構(gòu)參數(shù)

●反應(yīng)器:可適配光催化反應(yīng)器,、光電催化,、光熱催化反應(yīng)器;可根據(jù)實(shí)際實(shí)驗(yàn)需求定制;

●整機(jī)尺寸/mm:490 (L)×520 (W)×740 (H)

●金屬防護(hù)箱體:對(duì)輻射可能的氣體泄漏有一定防護(hù)作用

●光防護(hù)罩:便攜式光防護(hù)罩，可有效防止光污染

 

系統(tǒng)管路參數(shù)

●絕壓真空度:≤1.5 kPa

●使用壓力范圍:0 kPa~常壓

●閥門(mén)數(shù)量:7

●管路體積:65 mL,，系統(tǒng)富集能力強(qiáng)

●管路材質(zhì):高硼硅玻璃,，高化學(xué)惰性，無(wú)吸附

●閥門(mén)工藝：高硼硅玻璃材質(zhì),，閥塞與閥套采用對(duì)磨精磨工藝

●真空脂：進(jìn)口道康寧真空脂,，耐化學(xué)品的侵蝕，低蒸汽壓力,，低揮發(fā)性,，工作溫度：-40℃~200℃

●定量環(huán)：0.6 mL、2 mL可選,，系統(tǒng)靈敏度可調(diào)

●儲(chǔ)氣瓶：150 mL,，適用系統(tǒng)擴(kuò)容和反應(yīng)氣如二氧化碳的存儲(chǔ)

●管路控溫：循環(huán)管路及進(jìn)樣管路均可進(jìn)行控溫，最高可控200℃ ,；10段程序控溫,，控溫精度±0.1℃；

●冷凝管（球形/蛇形）：冷凝充分,，避免水蒸氣進(jìn)入氣相色譜儀和真空泵

●冷阱（選配）：分離低沸點(diǎn)組分,，延長(zhǎng)真空泵使用壽命,，提高系統(tǒng)真空度

控制單元參數(shù)

●軟件模塊：32位控制軟件和4.5寸TFF彩色觸摸屏 ；內(nèi)置儀器方法用于控制玻璃閥動(dòng)作,、氣相色譜儀及真空泵啟停,，操作簡(jiǎn)單；自動(dòng)控制模式下,，可實(shí)時(shí)顯示閥門(mén)位置,，具有安全防護(hù)預(yù)警功能；傳感器自動(dòng)提示更換真空脂,；具有二級(jí)加密調(diào)試程序,，用于設(shè)備調(diào)試、內(nèi)部方法設(shè)定及資深用戶靈活使用,；實(shí)時(shí)顯示系統(tǒng)內(nèi)部反應(yīng)壓力,、環(huán)境溫度等參數(shù)；

●自動(dòng)取樣閥：高硼硅玻璃材質(zhì),，內(nèi)置定量環(huán) ,；多通復(fù)合取樣閥，減少系統(tǒng)循環(huán)體積 ,；支持手動(dòng),、自動(dòng)、半自動(dòng)操作模式,；

●真空泵：系統(tǒng)控制軟件自動(dòng)控制啟停,，間歇式工作，噪音??； 含單向電磁閥，可防止泵油倒吸,；

檢測(cè)參數(shù)

●檢測(cè)范圍：H2,、O2、CH4,、CO等多種微量氣體,；

●檢出限/μmol：H2：0.05；O2：0.1,；CH4/CO：0.0005,。

代表文獻(xiàn)

華東理工大學(xué)李春忠團(tuán)隊(duì)引用Labsolar-6A光催化反應(yīng)系統(tǒng)

青島科技大學(xué)李鎮(zhèn)江團(tuán)隊(duì)引用Labsolar-6A光催化反應(yīng)系統(tǒng).png

陜西師范大學(xué)蔣加興團(tuán)隊(duì)引用Labsolar-6A光催化反應(yīng)系統(tǒng)

陜西師范大學(xué)劉生忠團(tuán)隊(duì)引用Labsolar-6A光催化反應(yīng)系統(tǒng)

應(yīng)化所王穎團(tuán)隊(duì)引用Labsolar-6A光催化反應(yīng)系統(tǒng)

深圳大學(xué)團(tuán)隊(duì)引用Labsolar-6A全玻璃微量氣體分析系統(tǒng).png

  • 膜光催化
  • 光降解氣體污染物
  • 光熱催化（負(fù)壓常壓體系）
  • PEC光電化學(xué)
  • 光催化量子效率測(cè)量
  • 電化學(xué)
  • 光催化二氧化碳還原
  • 光催化全分解水
  • 光催化分解水制氫/氧
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